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Beilstein J. Org. Chem. 2016, 12, 328–333, doi:10.3762/bjoc.12.35
Graphical Abstract
Figure 1: Structure of mycothiol 1.
Scheme 1: Detoxification pathway mediated by MSH.
Scheme 2: Anomerization via endocyclic cleavage.
Scheme 3: Outline of mycothiol synthesis by anomerization.
Scheme 4: Synthesis of a pseudodisaccharide by an anomerization reaction.
Scheme 5: Mycothiol synthesis from pseudo-disaccharide 4.
Beilstein J. Org. Chem. 2012, 8, 456–460, doi:10.3762/bjoc.8.52
Scheme 1: Electrochemical conversion of thioglycosides to glycosyl triflates.
Figure 1: 1H NMR spectrum of glycosyl triflate 2a.
Scheme 2: Triflic acid mediated isomerization of β-glycoside.